Welcome to the Wake Forest
University Regional Microscopy Facility. This user
facility serves the research community of Wake Forest University
as
well as the research and engineering communities of the western
Carolinas. The facility specializes in advanced
imaging techniques for biological and bio-medically relevant materials,
composite materials, interfaces, polycrystalline materials, and
nanophase materials. We are housed in two laboratories: the Deacon
Blvd. research facility and the
Hanes
Building on the Bowman Gray Campus. The facility offers HRTEM, CTEM, FE-SEM, SEM, and a
variety of scanning probe microscopies.
The facility is
managed by the Center
for Nanotechnology and Molecular Materials at Wake
Forest University
Electron Microscopy
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Philips
CM30
- High-resolution bright- and dark-field imaging
- TEM microprobe and nanoprobe analysis
- Small-probe convergent beam
- Large specimen tilt compatible with high resolution
- Sample size: 3 mm discs < 1 mm thick
- Point-point resolution: 0.23 nm
- Line resolution: 0.2 nm
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Jeol 1200 EX
- Resolution 0.45 nm point to point
- 300,000X magnification
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Field Emission Scanning
Electron Microscopy (FE-SEM)
Jeol JSM 6330
- Cold
field emission scanning electron microscope.
- High brightness (large current density) and small
beam diameter (high resolution) at low accelerating voltages.
- Resolution ~ 15 Angstroms depending on the
sample.
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Scanning Probe Microscopy
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Jeol 5200
(Description
from the Jeol web site)
The JSPM-5200 can be
configured as either an atomic force microscope (AFM) or
scanning tunneling microscope ( STM ) by merely changing the
tip. STM modes include CITS, I-V, S-V, and I-S. Standard AFM
modes include contact, friction force microscopy, current image,
non-contact and discrete contact with either slope detection or
frequency detection, and phase imaging.
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Scanning Tunneling Microscopy (STM)
RHK
This microscope was developed in
cooperation with RHK Technology, Inc. It is
equipped with a cryostat. The ultra high vacuum system was custom
designed and
built by Duniway Stockroom Corp. Further, this STM uses quite low
tunneling
currents with imaging having been achieved at tunnel currents
below 1 pA. The system is ideal for studies of nanostructures
which might otherwise be damaged by the large field densities wihin the
tunneling junction. Modifications are constantly being made to
this machine as we develop new techniques for high precision
determinations of electronic phenomena in nanostructures.
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Optical Microscopy
Olympus BX-60M
Metallographic Microscope
12V, 100 W
Illumination System. Brightfield,
Darkfield, Reflected Light, Reflected/Transmitted Light, Polarized Light,
Nomarski DIC, Fluorescence
Olympus Vanox
Fluorescence Microscope
Condensers available for this microscope include brightfield
and
darkfield throughout the full range of optical corrections. Objectives
range from achromat through the high-end planapochromats at
magnification factors between 1x and 150x.



Using
the Facility
Facility hours of operation are
9:00 am to 4:00 pm M-F.
Charges:
| Microscope |
Charge for external users |
Charge for WFU users |
Supplies that must be purchased |
| HRTEM, |
$100/hour |
$50/hour |
grids (film is optional) |
| CTEM |
$100/hour |
$50/hour |
grids/film/developer |
| FE-SEM |
$100/hour |
$50/hour |
sample mounts/conductive tape |
| AFM |
$50/hour |
$25/hour |
tips/sample mounts |
| STM |
$50/Hour |
$25/hour |
tips |
| Optical |
No Charge |
No Charge |
none |
| Individual training |
$150/hour |
$100/hour |
notebook |
| Users courses are offered each semester. Register through WFU or Forsyth Tech. |
Schedule by phone: 336 727 1806
Schedule by email: nanotech@wfu.edu
Schedule a training session or enroll in users course: carroldl@wfu.edu.
All users are required to assume a reasonable responsibility for personal safety, safety of facility personnel as it pertains to their use of the microscopes, and for the microscope being used.